Solid state amorphization of Fe50Nb50 powders during mechanical alloying

C. K. Lin, P. Y. Lee, S. W. Kao, G. S. Chen, R. F. Louh, Y. Hwu

Research output: Chapter in Book/Report/Conference proceedingChapter

4 Citations (Scopus)

Abstract

In the current study, the progress of solid state amorphization reaction of Fe50Nb50 alloy powders starting from elemental Fe and Nb powder mixtures by mechanical alloying was investigated. Techniques including scanning electron microscopy, microhardness, X-ray diffraction, differential thermal analysis, and extended X-ray absorption fine structure (EXAFS) were used to investigate the as-milled powders as a function of milling time. The intensities of the crystalline peaks of the elemental powders gradually decreased as the milling time increased and, after 15 hours of milling, an amorphous-indicating broad peak formed. The radial distribution functions obtained from Fourier transformation of EXAFS spectra reveal that there are differences in local atomic structure after prolonged milling. Combined with the information from various techniques, the amorphization process of Fe50Nb50 during MA is better understood.

Original languageEnglish
Title of host publicationMaterials Science Forum
PublisherTrans Tech Publ
Pages55-60
Number of pages6
Volume312
Publication statusPublished - 1999
Externally publishedYes
EventProceedings of the 1998 International Symposium on Metastable, Mechanical Alloyed and Nanocrystalline Materials, ISMANAM-98 - Wollongong, Sydney, Aust
Duration: Dec 7 1998Dec 12 1998

Other

OtherProceedings of the 1998 International Symposium on Metastable, Mechanical Alloyed and Nanocrystalline Materials, ISMANAM-98
CityWollongong, Sydney, Aust
Period12/7/9812/12/98

Fingerprint

Amorphization
Mechanical alloying
Powders
X ray absorption
Microhardness
Differential thermal analysis
Distribution functions
Crystalline materials
X ray diffraction
Scanning electron microscopy

ASJC Scopus subject areas

  • Materials Science(all)

Cite this

Lin, C. K., Lee, P. Y., Kao, S. W., Chen, G. S., Louh, R. F., & Hwu, Y. (1999). Solid state amorphization of Fe50Nb50 powders during mechanical alloying. In Materials Science Forum (Vol. 312, pp. 55-60). Trans Tech Publ.

Solid state amorphization of Fe50Nb50 powders during mechanical alloying. / Lin, C. K.; Lee, P. Y.; Kao, S. W.; Chen, G. S.; Louh, R. F.; Hwu, Y.

Materials Science Forum. Vol. 312 Trans Tech Publ, 1999. p. 55-60.

Research output: Chapter in Book/Report/Conference proceedingChapter

Lin, CK, Lee, PY, Kao, SW, Chen, GS, Louh, RF & Hwu, Y 1999, Solid state amorphization of Fe50Nb50 powders during mechanical alloying. in Materials Science Forum. vol. 312, Trans Tech Publ, pp. 55-60, Proceedings of the 1998 International Symposium on Metastable, Mechanical Alloyed and Nanocrystalline Materials, ISMANAM-98, Wollongong, Sydney, Aust, 12/7/98.
Lin CK, Lee PY, Kao SW, Chen GS, Louh RF, Hwu Y. Solid state amorphization of Fe50Nb50 powders during mechanical alloying. In Materials Science Forum. Vol. 312. Trans Tech Publ. 1999. p. 55-60
Lin, C. K. ; Lee, P. Y. ; Kao, S. W. ; Chen, G. S. ; Louh, R. F. ; Hwu, Y. / Solid state amorphization of Fe50Nb50 powders during mechanical alloying. Materials Science Forum. Vol. 312 Trans Tech Publ, 1999. pp. 55-60
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