Double-quantum NMR spectroscopy based on finite pulse RFDR

Yao Hung Tseng, Yun Mou, Chung Yuan Mou, Jerry C.C. Chan

Research output: Contribution to journalArticlepeer-review

24 Citations (Scopus)

Abstract

We demonstrate that the finite pulse RFDR sequence (J. Chem. Phys. 114 (2001) 8473) can be used effectively for 31P double-quantum NMR spectroscopy at a spinning frequency of 10 kHz. The 31P NMR data measured for hydroxyapatite and octacalcium phosphate show that sizable double-quantum excitation efficiency can be obtained with the ratio of the recoupling field to spinning frequency set equal to 1.67.

Original languageEnglish
Pages (from-to)266-270
Number of pages5
JournalSolid State Nuclear Magnetic Resonance
Volume27
Issue number4
DOIs
Publication statusPublished - Jun 2005
Externally publishedYes

Keywords

  • Double-quantum
  • DQ
  • fpRFDR
  • MAS
  • P-31 NMR

ASJC Scopus subject areas

  • Radiation
  • Chemistry(all)
  • Nuclear and High Energy Physics
  • Instrumentation

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